反应条件
in neat (no solvent) exclusion of moisture; platinum vessel; S2Br2 may contain sulfur (satd. soln.) or bromine (20percent); introduction of purified fluorine; ambient temp. or -30 or 120°C; detailed description of apparatus and handling given;; condensation, distillation; agitation in a platinum flask (glass or quartz cause formation of oxygen compounds), containing metallic mercury for removal of SF2/S2F2; distillation;;
参考文献
S: MVol.B3, 79, page 1706 - 1708
Diss. Breslau (1935) 1936, S. 17
Diss. Breslau (1935) 1936, S. 31
Diss. Breslau T. H. (1935) 1936, S. 11
