in neat (no solvent)
byproducts: CF4; introduction of F2 (from electrolysis/graphite anode); abs. exclusion of air (N2 atm.); detailed description of apparatus and handling given;; condensed (liquid air); storage over aq. KOH (for weeks); repeated fractionating (and drying); passing over liquid mixture of metallic Na/K (removal of SO2F2;;
参考文献
Denbigh, K. G.; Whytlaw-Gray, R.
Journal of the Chemical Society, 1934 , p. 1346 - 1352
in neat (no solvent)
passing F2 over sulfur;; cooled (liquid air); fractionated;;
参考文献
Denbigh, K. G.; Whytlaw-Gray, R.
Journal of the Chemical Society, 1934 , p. 1346 - 1352
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Gmelin Handbook: S: MVol.B3, 75, page 1698 - 1701
