in neat (no solvent) reaction with pure dry C2H2 at 250-300°C;; purification by fractionated distillation;;
参考文献
Mazza, F. P.; Solazzo, L.
Rendiconto dell'Accademia delle Scienze Fisiche e Matematiche, Naples, 1927 , vol. 33, p. 236 - 236
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Gmelin Handbook: Se: MVol.A1, 79, page 254 - 257
in neat (no solvent) mixt. heated (600°C, 12 h) in evacuated silica ampule; homogenized in rocking furnace; quenched in air; annealed near glass transition temp.; XRD;
参考文献
Banser, Deike; Schnell, Melanie; Grabow, Jens-Uwe; Cocinero, Emilio J.; Lesarri, Alberto; Alonso, Jose L.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 39 p. 6311 - 6315