硝酸铁(III) 九水合物合成路线 (共 31 条)
反应条件
in neat (no solvent)
参考文献
Gmelin Handbook: Hg: MVol.B3, 6.16, page 1249 - 1262
反应条件
in water evapn. of soln. Fe(NO3)3 and H3PO4, annealing (400°C, N2 atmosphere, 24 h);
参考文献
Malaman, B.; Ijjaali, M.; Gerardin, R.; Venturini, G.; Gleitzer, C.
European Journal of Solid State and Inorganic Chemistry, 1992 , vol. 29, p. 1269 - 1284
反应条件
in water 4 h; Product distribution / selectivity;
参考文献
Hsiao, Yih-Ming; Chiu, Hsueh-Hung; Wang, Hsiu-Ching; Chang, Yu-Chen
Patent: US2005/80283 A1, 2005 ;
Location in patent: Page/Page column 2 ;
反应条件
1: T=450°C; 8 h; 2: With hydrogen T=500°C; 16 h;
参考文献
Szegedi, Agnes; Hegedus, Mihaly; Margitfalvi, Jozsef L.; Kiricsi, Imre
Chemical Communications, 2005 , # 11 p. 1441 - 1443
反应条件
hydrogen in water NH4OH added to aq. Fe(NO3)3, ppt. calcined at 400°C for 3 h, crushed into fine powder, rubbed onto KBr disk, evacuated for 5 h at room temp., reduced for 120 h at 400°C in stream of H2;
参考文献
Kotanigawa, Takeshi; Shimokawa, Katsuyoshi; Yamamoto, Mitsuyoshi
Journal of the Chemical Society, Chemical Communications, 1982 , # 1 p. 29 - 30
参考文献
Gmelin Handbook: Na: SVol.3, 1.5.5, page 947 - 953
反应条件
oxalic acid in water
byproducts: CO2; react. of an aq. Fe(NO3)3 soln. with oxalic acid; evolution of CO2 and NO2; first formation of basic iron(III)nitrate oxide, then iron oxide;; pptn.;;
参考文献
Gmelin Handbook: Fe: MVol.B1, 75, page 170 - 172
参考文献
Gmelin Handbook: N: MVol.3, 4.2, page 757 - 764
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Kali-Forschungs-Anstalt
Patent: DE540206 , 1930 ;
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Kali-Forschungs-Anstalt
Patent: FR39294 , 1930 ;
反应条件
ammonium hydroxide; ammonium nitrate; ammonium chloride; ammonia; sodium in tetrahydrofuran
参考文献
Hoechst-Roussel Pharmaceuticals Incorporated
Patent: US4521537 A1, 1985 ;
反应条件
sodium; acetic acid in water
参考文献
Roussel Uclaf
Patent: US4304733 A1, 1981 ;