in diethyl ether diethyl ether added to mixture of MgCl2 and alanate, suspn. stirred under reflux for 8 h, storage overnight; evapd., extd. with diethyl ether several days; elem. anal., XRD;
参考文献
Journal of Alloys and Compounds, , vol. 345, # 1-2 p. 286 - 296
→
反应条件
in solid (Ar) mixt. milled for 3 h; according to M. Mamatha, B. Bogdanovic, M. Felderhoff, A. Pommerin, W. Schmidt, F. Schueth, C. Weidenhalter, J. AlloyCompd. web release 22 August 2005; detn. by XRD, DSC;
参考文献
Fossdal; Brinks; Fichtner; Hauback
Journal of Alloys and Compounds, 2005 , vol. 387, # 1-2 p. 47 - 51
Gmelin Handbook: U: SVol.C8, 5.1.2, page 12 - 55
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Katz, J. J.; Rabinowitch, E.
The Chemistry of Uranium, Tl.1, McGraw-Hill, New York - Toronto - London 1951, S.355/82
Archambault, J. D.; Sisler, H. H.; Ryschkewitsch, G. E.
Journal of Inorganic and Nuclear Chemistry, 1961 , vol. 17, p. 130 - 134
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
in neat (no solvent)
byproducts: C, NaCl; mixtures of MgCl2 and NaCN formed on heating at temp. above 500 °C quantitative MgCN2, further increase of the temp. started N2 evolution started and the yield of MgCN2 decreased;;
参考文献
Perret; Perrot
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1936 , vol. 202, p. 422
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Gmelin Handbook: Mg: MVol.B1, 53, page 111 - 113
