1,1-dibromo ethane in tetrahydrofuran Kinetics; (Ar or vac.); a soln. of Sn compd. in THF kept over Mg turnings (preactivated with dibromoethane) at 293 K for 48 h under stirring;
参考文献
Russian Journal of General Chemistry, , vol. 74, # 7 p. 1101 - 1104
in neat (no solvent) byproducts: CO, CO2, Cl2; a stream of N2 containing CCl4 was passed over heated MgO forming MgCl2, MgCO3, CO, CO2, Cl2 and COCl2;;
参考文献
Memoire Presente a la Faculte des Sciences de l'Universite de Paris pour l'Obtention du Diplome d'Etudes Superieures, Paris 1934, S. 14
in neat (no solvent) byproducts: C, Mg-carbide; in H2 atmosphere start of reaction at gentle heating with deposition of C; at red heat vigorous reaction;;
参考文献
Liebigs Annalen der Chemie, , vol. 267, p. 234 - 234