in water-d2 over 1 h at 30°C; not isolated, detected by NMR;
参考文献
Dixon, Nicholas E.; Jackson, W. Gregory; Lancaster, Martin J.; Lawrance, Geoffrey A.; Sargeson, Alan M.
Inorganic Chemistry, 1981 , vol. 20, p. 470 - 476
in further solvent(s) further solvent=benzoylchloride; dropwise addn. of D2O to benzoyl chloride, passing gases through ice cooled tube, absorption in pure H2O, rinsing with air;;
in neat (no solvent) according to: D. P. Shoemaker, C. W. Garland, J. W. Nibler, Experiments in Physical Chemistry, fifth edition, McGraw-Hill, New York, 1989; cryogenic distn. with liquid nitrogen;
参考文献
Elrod, Matthew J.; Host, Bryan C.; Steyert, David W.; Saykally, Richard J.
Molecular Physics, 1993 , vol. 79, p. 245 - 252
in neat (no solvent) in vac. (<10 mTorr); repeated distn. from ethanol (slush temp. -117 to -196°C); IR;
参考文献
Husain, David; Plane, John M. C.; Xiang, Chen Cong
Journal of the Chemical Society, Faraday Transactions 2: Molecular and Chemical Physics, 1984 , vol. 80, p. 713 - 728
