反应条件
in neat (no solvent) degassed ICl was treated with excess of Cl2 at ca. -50°C in the small greasless reactor, the reactor was warm up to room temp. for 30 min; excess of Cl2 was removed under vac. at -50;
参考文献
Kuvychko, Igor V.; Streletskii, Alexey V.; Shustova, Natalia B.; Seppelt, Konrad; Drewello, Thomas; Popov, Alexey A.; Strauss, Steven H.; Boltalina, Olga V.
Journal of the American Chemical Society, 2010 , vol. 132, # 18 p. 6443 - 6462
