in water
at ambient temp. slow, at heating vigorous reaction;;
参考文献
Henry, L.
Ber., 1870 , vol. 3, p. 892 - 892
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Henry, L.
Bulletin de la Societe Chimique de France, 1871 , vol. 15, p. 28 - 28
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Gmelin Handbook: I: MVol.2, 173, page 628 - 629
Henry, L.
Ber., 1870 , vol. 3, p. 892 - 892
Full Text Show Details
Henry, L.
Bulletin de la Societe Chimique de France, 1871 , vol. 15, p. 28 - 28
Full Text Show Details
Gmelin Handbook: I: MVol.2, 173, page 628 - 629
in tetrachloromethane; dichloromethane
solution of ICl (1.32 mmol) in CCl4 was added dropwise (0,5 h) to a stirred solution of tin compound (1.26 mmol) in 1/4 CH2Cl2/CCl4 at room temperature; reaction was monitored by (1)H-NMR spectroscopy; solvent was removed under reduced pressure; pink residue kept under vacuum for 3 h; product was identified by comparison of its spectra with an authentic sample;
参考文献
Dhaher, Saadi M.; Eaborn, Colin; Smith, J. David
Journal of Organometallic Chemistry, 1988 , vol. 355, p. 33 - 44