in sulfuryl dichloride conversion of SnCl4 with SO3 in 20- respectively 5percent solns. of SO2Cl2 (exothermic reaction); molar ratio (SnCl4:SO3) = 1:0.5-2;; washing of crystals in SO2Cl2; drying in a vacuum;;
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Gmelin Handbook: Sn: MVol.C2, 9.32, page 77 - 77
Dillamore, I. M.; Edwads, D. A.
J. Inorg. Chem., 1969 , vol. 31, p. 2427 - 2430
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Gmelin Handbook: Os: SVol.1, 1.4, page 18 - 19