(4-甲基磺酰基苯基)-磷酸二乙酯合成路线 （共 5 条）
反应条件
α-cyclohexylcyclohexanemethanamine; triphenylphosphine; palladium diacetate in ethanol
T=76°C; 16 h;
参考文献
Goossen, Lukas J.; Dezfuli, Mohammad K.
Synlett, 2005 , # 3 art. no. G45204ST, p. 445 - 448
反应条件
nickel dichloride
T=180°C; 0.5 h;
参考文献
Grabiak, Raymond C.; Miles, James A.; Schwenzer, Gretchen M.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 197 - 202
反应条件
1: 82 percent / PCl3, BiCl3 / 2.5 h / Heating
2: 1.) sodium ethylate, 2.) I2 / 1) 1 h; 2) 2 h
View Scheme
参考文献
Simeon, Fabrice; Jaffres, Paul-Alain; Villemin, Didier
Tetrahedron, 1998 , vol. 54, # 34 p. 10111 - 10118
反应条件
iodine; sodium ethanolate
1) 1 h; 2) 2 h; Yield given. Multistep reaction;
参考文献
Simeon, Fabrice; Jaffres, Paul-Alain; Villemin, Didier
Tetrahedron, 1998 , vol. 54, # 34 p. 10111 - 10118
反应条件
hydrogenchloride
8 h; Heating;
参考文献
Grabiak, Raymond C.; Miles, James A.; Schwenzer, Gretchen M.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 197 - 202
