(2-甲基-5,6,7,8-四氢-[1]苯并噻吩并[3,2-e]嘧啶-4-基)肼合成路线 (共 10 条)
反应条件
hydrazine hydrate in ethanol
2 h; Heating;
参考文献
Shishoo, C. J.; Devani, M. B.; Karvekar, M. D.; Ullas, G. V.; Ananthan, S.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. <B> 21, # 7 p. 666 - 668
反应条件
1: 80 percent / HClgas / dioxane / 5 h
2: 68 percent / POCl3 / 12 h / Heating
3: 88 percent / NH2NH2*H2O / ethanol / 2 h / Heating
View Scheme
参考文献
Shishoo, C. J.; Devani, M. B.; Karvekar, M. D.; Ullas, G. V.; Ananthan, S.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. <B> 21, # 7 p. 666 - 668
反应条件
1: 68 percent / POCl3 / 12 h / Heating
2: 88 percent / NH2NH2*H2O / ethanol / 2 h / Heating
View Scheme
参考文献
Shishoo, C. J.; Devani, M. B.; Karvekar, M. D.; Ullas, G. V.; Ananthan, S.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. <B> 21, # 7 p. 666 - 668
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
反应条件
1: 6 h / 40 - 50 °C
2: p-toluenesulfonic acid / benzene / 4 h / Heating
View Scheme
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
参考文献
Shishoo, C. J.; Devani, M. B.; Ullas, G. V.; Anathan, S.; Bhadti, V. S.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 43 - 46
反应条件
aq. 2 in acetic acid
T=5°C;
参考文献
Shishoo, C. J.; Devani, M. B.; Karvekar, M. D.; Ullas, G. V.; Ananthan, S.; et al.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. <B> 21, # 7 p. 666 - 668