in Petroleum ether dropwise addn. of soln. of SnCl4 in petroleum ether (40-60°C) to soln. of 1-trialkoxysilyl 2-phenylhydrazine (equimolar amts., 0 to -10°C, under dry nitrogen), ppt. filtered in a cold atm. of dry N2; washed, dried under reduced pressure; elem. anal.;
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 1 p. 148 - 151
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 170 - 173
in Petroleum ether dropwise addn. of soln. of TiCl4 in petroleum ether (40-60°C) to soln. of 1-trialkoxysilyl 2-phenylhydrazine (equimolar amts., 0 to -10°C, under dry nitrogen), ppt. filtered in a cold atm. of dry N2; washed, dried under reduced pressure; elem. anal.;
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 1 p. 148 - 151
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 1 p. 170 - 173