反应条件
1: With bis(cyclopentadienyl)titanium dichloride; 2,3,5,6-tetramethyl-1,4-bis(trimethylsilyl)-1,4-diaza-2,5-cyclohexadiene in tetrahydrofuran
T=20°C; Reformatsky Reaction; 14 h; Inert atmosphere;
2: With hydrogenchloride in tetrahydrofuran; diethyl ether
Inert atmosphere;
参考文献
Saito, Teruhiko; Nishiyama, Haruka; Tanahashi, Hiromasa; Kawakita, Kento; Tsurugi, Hayato; Mashima, Kazushi
Journal of the American Chemical Society, 2014 , vol. 136, # 13 p. 5161 - 5170