triethylamine; sodium iodide; magnesium chloride in acetonitrile T=25°C; 3 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tirpak, Robin E.; Olsen, Richard, S.; Rathke, Michael W.
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4877 - 4879
Fischer
Diss.<Karlsruhe 1954>S.18-21
Full Text Show Details
Petrow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 1091,1094;engl.Ausg.S.1053,1056
ammonia; hydrogen; [RhCl(η2:η2-cycloocta-1,5-diene)]2; 2,2'-bis[[bis(3-sulfophenyl)phosphino]methyl]-4,4',7,7'-tetrasulfo-1,1'-binaphthyl octasodium salt in water T=100°C; P=47254.7 Torr; 7 h; Product distribution / selectivity;
参考文献
Degussa AG
Patent: US6884887 B1, 2005 ;
Location in patent: Page/Page column 10 ;
ammonia; hydrogen; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 2,2'-bis[[bis(3-sulfophenyl)phosphino]methyl]-4,4',7,7'-tetrasulfo-1,1'-binaphthyl octasodium salt in water T=130°C; P=82508.3 Torr; 5 h; Product distribution / selectivity;
参考文献
Degussa AG
Patent: US6884887 B1, 2005 ;
Location in patent: Page/Page column 10 ;
