反应条件
in tetrahydrofuran; water aq. hydroxylamine dissolved in THF, treated dropwise with 1-2 equiv. of CS2 at ice temp., warmed to room temp. over 45 min, stirred at room temp. for 3 h (mechanism discussed); ppt. filtered, kept at 7°C for 4 d, pptd., washed (ethyl acetate), dried (vac.);
参考文献
Inorganic Chemistry Communications, , vol. 13, # 5 p. 622 - 624
