in methanol; dichloromethane byproducts: (C6H5)3PO; N2 atmosphere; addn. of N2H4*H2O in CH3OH/CH2Cl2 to the Rh complex; stirring for 3 h;; the pptd. hydrido complex was filtered off; pptn. of the hydrazine complex by addn. of n-hexane to the filtrate; filtration; washing with n-hexane; elem. anal.;;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 20, # 7 p. 673 - 676
in methanol; dichloromethane byproducts: (C6H5)3PO; N2 atmosphere; addn. of N2H4*H2O in CH3OH/CH2Cl2 to the Rh complex; stirring for 3 h;; the pptd. hydrido complex was filtered off; pptn. of the hydrazine complex by addn. of n-hexane to the filtrate; filtration; washing with n-hexane; elem. anal.;;
参考文献
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, , vol. 20, # 7 p. 673 - 676
