in neat (no solvent)
heating with SO2(NH2)2 at 90 °C;; quantitative react.;;
参考文献
Kirsanov, A. V.
Zh. obshch. Khim., 1952 , vol. 22, p. 1346 - 1349
C., 1956 , p. 1242
Full Text Show Details
Gmelin Handbook: P: MVol.C, 192, page 441 - 443
in neat (no solvent)
heating a mixt. of SO2(NH2)2 and PCl5 with a reflux condenser at 60 and 90 °C;; removal of an excess of PCl4 on heating at 8 Torr and 100 °C for 1 h; recrystn. from C6H6;;
参考文献
Ephraim, F.; Gurewitsch, M.
Ber., 1910 , vol. 43, p. 138 - 148
HCl in water
boiling with dild. HCl soln.; formation of HSO3NH2 fast, further hydrolysis slow;;
参考文献
Traube, W.
Ber., 1893 , vol. 26, p. 607 - 613
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 35, page 1604 - 1606
Full Text Show Details
Mann, F. G.
Journal of the Chemical Society, 1933 , p. 412 - 419
HCl in water
boiling with dild. HCl soln.; formation of HSO3NH2 fast, further hydrolysis slow;;
参考文献
Traube, W.
Ber., 1893 , vol. 26, p. 607 - 613
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 35, page 1604 - 1606
Full Text Show Details
Mann, F. G.
Journal of the Chemical Society, 1933 , p. 412 - 419