1: 6-bromo-2-hydroxy-naphthalene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 5 h; Inert atmosphere; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-50°C; 0.75 h; Inert atmosphere;
参考文献
Verga, Daniela; Nadai, Matteo; Doria, Filippo; Percivalle, Claudia; Di Antonio, Marco; Palumbo, Manlio; Richter, Sara N.; Freccero, Mauro
Journal of the American Chemical Society, 2010 , vol. 132, # 41 p. 14625 - 14637
ethyl mercaptan sodium salt in N,N-dimethyl-formamide 0.333333 h; Heating;
参考文献
Schmidt, Jonathan M.; Tremblay, Gilles B.; Plastina, Michael A.; Ma, Fupeng; Bhal, Sanjivanjit; Feher, Miklos; Dunn-Dufault, Robert; Redden, Peter R.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 5 p. 1819 - 1828
1: With n-butyllithium in tetrahydrofuran T=-78 - -64°C; 0.416667 h; 2: With N,N-dimethyl-formamide in tetrahydrofuran T=-78 - 20°C; 1.33333 h; 3: With citric acid in tetrahydrofuran pH=5; 0.5 h;
