2-氨基-7-甲基-9H-硫代-9-噻吨酮合成路线 （共 7 条）
反应条件
hydrogenchloride; tin(ll) chloride in acetic acid Heating;
参考文献
Arur, P. V.; Kulkarni, Sheshgiri N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 1 p. 50 - 52
反应条件
1: 1) anhyd. K2CO3 / 1) water, methanol, reflux, 2) methanol, 10 h, reflux 2: 72 percent / conc. H2SO4 / 100 - 105 °C 3: 75 percent / stannous chloride, conc. HCl / acetic acid / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 1 p. 50 - 52
反应条件
1: 72 percent / conc. H2SO4 / 100 - 105 °C 2: 75 percent / stannous chloride, conc. HCl / acetic acid / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 1 p. 50 - 52
反应条件
1: 1) anhyd. K2CO3 / 1) water, methanol, reflux, 2) methanol, 10 h, reflux 2: 72 percent / conc. H2SO4 / 100 - 105 °C 3: 75 percent / stannous chloride, conc. HCl / acetic acid / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 20, # 1 p. 50 - 52
反应条件
1: thionyl chloride; benzene / Behandeln des Reaktionsprodukts mit Aluminiumchlorid in Nitrobenzol 2: acetic acid; tin (II)-chloride; aqueous hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , p. 757,761
反应条件
1: aqueous KOH 2: thionyl chloride; benzene / Behandeln des Reaktionsprodukts mit Aluminiumchlorid in Nitrobenzol 3: acetic acid; tin (II)-chloride; aqueous hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , p. 757,761
参考文献
Journal of the Chemical Society, , vol. 99, p. 2050
