N-甲氧基-N-甲基乙酰胺合成路线 （共 87 条）
反应条件
triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Kerr, William J.; Morrison, Angus J.; Pazicky, Marek; Weber, Tina
Organic Letters, 2012 , vol. 14, # 9 p. 2250 - 2253
反应条件
1: in tetrahydrofuran; toluene T=-30°C; 2 h; 2: With acetic anhydride in tetrahydrofuran; toluene T=-30°C; 0.5 h; 3: With ammonium chloride in tetrahydrofuran; water; toluene T=-30 - 10°C;
参考文献
Kuethe, Jeffrey T.; Yin, Jingjun; Huffman, Mark A.; Journet, Michel
Patent: US2007/15923 A1, 2007 ;
Location in patent: Page/Page column 8; 9 ;
反应条件
1: O,N-dimethyl-hydroxylamine hydrochloride With diisobutylaluminium hydride in tetrahydrofuran; toluene 2: acetic acid n-butyl ester in tetrahydrofuran T=20°C; 2 h;
参考文献
Huang, Pei-Qiang; Zheng, Xiao; Deng, Xian-Ming
Tetrahedron Letters, 2001 , vol. 42, # 51 p. 9039 - 9041
反应条件
1: 4,4,4-trifluoro-1-(N-methoxy-N-methylamino)-1-methyl-1-(trimethylsiloxyl)-2-butyne With tetrabutyl ammonium fluoride in tetrahydrofuran; diethyl ether T=-15°C; 0.166667 h; 2: 2,2,2-Trifluoro-1-phenyl-ethanone in tetrahydrofuran; diethyl ether T=20°C; 1 h;
参考文献
Jeong, In Howa; Jeon, Sung Lan; Kim, Bum Tae
Tetrahedron Letters, 2003 , vol. 44, # 38 p. 7213 - 7216
反应条件
1: With 3-hydroxybenzenethiol; potassium carbonate in N,N-dimethyl-formamide T=23°C; 2 h; 2: With tetra-(n-butyl)ammonium iodide; potassium carbonate; Merrifield resin in N,N-dimethyl-formamide T=50°C; 2 h; 3: With 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene-d6 T=150°C; 0.166667 h; microwave irradiation;
参考文献
Chemistry - A European Journal, , vol. 11, # 17 p. 4935 - 4952
反应条件
ozone in dichloromethane T=0°C;
参考文献
Tetrahedron, , vol. 53, # 15 p. 5463 - 5470
反应条件
ozone in dichloromethane T=0°C;
参考文献
Tetrahedron, , vol. 53, # 15 p. 5463 - 5470
反应条件
in water T=20°C; 17 h;
参考文献
Khodot; Petrova; Anikin; Chlenov
Russian Chemical Bulletin, 1996 , vol. 45, # 3 p. 727 - 729
反应条件
1: acetic acid With 1,1'-carbonyldiimidazole in dichloromethane T=0 - 23°C; 2: O,N-dimethyl-hydroxylamine hydrochloride With triethylamine in dichloromethane T=0°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 50, # 7 p. 781 - 784
反应条件
ozone in pentane T=0°C; Yields of byproduct given;
参考文献
Griesbaum, Karl; Liu, Xuejun; Kassiaris, Athanassios; Scherer, Martin
Liebigs Annales, 1997 , # 7 p. 1381 - 1390
