(2E)-2-丁烯-1,1-二醇二乙酸酯合成路线 (共 12 条)
反应条件
palladium diacetate; 1,2-bis-(diphenylphosphino)ethane 1.) THF, reflux, 2.) 100 degC, 2 h, water; Yield given. Multistep reaction;
参考文献
Lu, Xiyan; Huang, Yujin
Tetrahedron Letters, 1986 , vol. 27, # 14 p. 1615 - 1616
反应条件
diarsenic pentoxide; sulfuric acid
参考文献
Case
Journal of the American Chemical Society, 1948 , vol. 70, p. 3994
反应条件
sulfuric acid; nitrobenzene
参考文献
Utermohlen
Journal of Organic Chemistry, 1943 , vol. 8, p. 544,546
反应条件
ethanol T=50°C; 0.166667 h; chemoselective reaction;
参考文献
Massah, Ahmad Reza; Kalbasi, Roozbeh Javad; Shafiei, Anahita
Monatshefte fur Chemie, 2012 , vol. 143, # 4 p. 643 - 652
参考文献
Lagermark; Eltekow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1879 , vol. 11, p. 79
参考文献
I.G. Farbenind.
Patent: DE719571 , 1938 ;
DRP/DRBP Org.Chem.
反应条件
diarsenic pentoxide; sulfuric acid
参考文献
Utermohlen
Journal of Organic Chemistry, 1943 , vol. 8, p. 544,546
参考文献
I.G. Farbenind.
Patent: DE719571 , 1938 ;
DRP/DRBP Org.Chem.
反应条件
titanium tetrachloride in dichloromethane
T=-78 - 20°C; Substitution;
参考文献
Sandberg, Marcel; Sydnes, Leiv K.
Organic Letters, 2000 , vol. 2, # 5 p. 687 - 689
反应条件
in dimethyl sulfoxide
T=20°C; Substitution;
参考文献
Sandberg, Marcel; Sydnes, Leiv K.
Organic Letters, 2000 , vol. 2, # 5 p. 687 - 689