4-(4-甲氧基苯氧基)苯甲腈合成路线 （共 17 条）
反应条件
tetrabutylammomium bromide; caesium carbonate in 1-methyl-pyrrolidin-2-one; n-hexyl ether
T=120°C; Ullmann reaction; 12 h; Inert atmosphere;
参考文献
Yang, Shuliang; Wu, Cunqi; Zhou, Hua; Yang, Yanqin; Zhao, Yongxia; Wang, Chenxu; Yang, Wei; Xu, Jingwei
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 53 - 58
反应条件
copper(l) iodide; glycine-N',N'-dimethylamide hydrochloride; caesium carbonate in 1,4-dioxane
T=90°C;
参考文献
DECODE CHEMISTRY, INC.
Patent: US2007/66820 A1, 2007 ;
Location in patent: Page/Page column 26 ;
US 20070066820 A1
反应条件
potassium fluoride on basic alumina; 18-crown-6 ether in dimethyl sulfoxide
T=140°C; 3 h;
参考文献
Islam, Sk.Manirul; Mondal, Sanchita; Mondal, Paramita; Roy, Anupam Singha; Tuhina; Salam, Noor; Mobarak, Manir
Journal of Organometallic Chemistry, 2012 , vol. 696, # 26 p. 4264 - 4274
反应条件
P(i-BuNCH2CH2)3N in N,N-dimethyl-formamide; toluene
T=80°C; 3 h;
参考文献
Raders, Steven M.; Verkade, John G.
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3507 - 3511
反应条件
potassium carbonate in dimethyl sulfoxide
0.0833333 h; Heatingmicrowave irradiation;
参考文献
Li, Feng; Meng, Qingqing; Chen, Huansheng; Li, Zhiming; Wang, Quanrui; Tao, Fenggang
Synthesis, 2005 , # 8 art. no. F13304SS, p. 1305 - 1313
反应条件
carbon dioxide; tetrabutylammomium bromide; cesium fluoride
T=110°C; P=172517 Torr;
参考文献
Lee, Jin-Kyun; Fuchter, Matthew J.; Williamson, Rachel M.; Leeke, Gary A.; Bush, Edward J.; McConvey, Ian F.; Saubern, Simon; Ryan, John H.; Holmes, Andrew B.
Chemical Communications, 2008 , # 39 p. 4780 - 4782
反应条件
potassium phosphate in tetrahydrofuran
T=115°C; 18 h;
参考文献
Ghosh, Rajshekhar; Samuelson, Ashoka G.
New Journal of Chemistry, 2004 , vol. 28, # 11 p. 1390 - 1393
反应条件
[Pd((.eta.5-C5H5)Fe[(.eta.5-C5H3)C(Me)=N(C6H4-4-Me)])(.mu.-Cl)]2; caesium carbonate in N,N-dimethyl-formamide
T=100°C; 2 h;
参考文献
Wang, Hailei; Yu, Ajuan; Cao, Aijuan; Chang, Junbiao; Wu, Yangjie
Applied Organometallic Chemistry, 2013 , vol. 27, # 10 p. 611 - 614
反应条件
potassium carbonate in dimethyl sulfoxide
0.0833333 h; microwave irradiation;
参考文献
Dey, Archan; Desiraju, Gautam R.
Chemical Communications, 2005 , # 19 p. 2486 - 2488
反应条件
potassium carbonate in dimethyl sulfoxide
0.0833333 h; microwave irradiation;
参考文献
Dey, Archan; Desiraju, Gautam R.
Chemical Communications, 2005 , # 19 p. 2486 - 2488
