N-(4-甲基苯基)-N-[(E)-3-(4-甲基苯基)亚氨基丙-1-烯基]苯甲酰胺合成路线 （共 9 条）
反应条件
1: 10 mg / 0.1 N HCl / tetrahydrofuran; diethyl ether / 0.27 h / Ambient temperature 2: 51 percent / CH2Cl2 / 2 h / Ambient temperature 3: 10 mg / AcOH, AcONa.3H2O, H2O, 7percent NaHCO3, HCl / dioxane / 3.5 h / 100 °C View Scheme
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
1: 0.73 g / 7percent NaHCO3 / tetrahydrofuran; methanol / 24 h / Ambient temperature 2: 51 percent / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
hydrogenchloride in tetrahydrofuran; diethyl ether 0.266667 h; Ambient temperature;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 4 p. 1443 - 1452
反应条件
sodium hydroxide in water T=60°C; 9 h; other derivatives of malonaldehyde dianil investigated; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 2 p. 308 - 317
反应条件
1: 10 mg / 0.1 N HCl / tetrahydrofuran; diethyl ether / 0.27 h / Ambient temperature
2: 51 percent / CH2Cl2 / 2 h / Ambient temperature
3: 1.43 g / AcOH, AcONa.3H2O, H2O, 7percent NaHCO3, HCl / dioxane / 3.5 h / 100 °C
View Scheme
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1453 - 1462
反应条件
sodium hydroxide in water
T=60°C; 9 h; other derivatives of malonaldehyde dianil investigated; Product distribution;
参考文献
Tamura; Ono
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 2 p. 308 - 317
反应条件
1: 90 mg / 0.1 N HCl / tetrahydrofuran; diethyl ether / 0.27 h / Ambient temperature
2: 43 mg / benzene / 13 h / 85 °C
3: 8 mg / 0.1 N NaOH, 7percent NaHCO3 / dioxane; H2O / 48 h / Ambient temperature
View Scheme
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1443 - 1452
反应条件
sodium hydrogencarbonate in tetrahydrofuran; methanol
24 h; Ambient temperature;
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1443 - 1452
反应条件
sodium hydrogencarbonate in tetrahydrofuran; methanol
24 h; Ambient temperature;
参考文献
Ono, Machiko; Tamura, Shinzo
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 4 p. 1443 - 1452
