四乙基氟代亚甲基二磷酸酯合成路线 （共 13 条）
反应条件
trimethylsilyl bromide 72 h; Ambient temperature;
参考文献
Hamilton, Chris J.; Roberts, Stanley M.; Shipitsin, Alexander
Chemical Communications, 1998 , # 10 p. 1087 - 1088
反应条件
sodium hydride; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in tetrahydrofuran
T=0 - 20°C;
参考文献
Cui, Peng; McCalmont, William F.; Tomsig, Jose L.; Lynch, Kevin R.; Macdonald, Timothy L.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 5 p. 2212 - 2225
反应条件
hydrogenchloride in water
参考文献
Iorga, Bogdan; Eymery, Frederic; Savignac, Philippe
Tetrahedron Letters, 1998 , vol. 39, # 25 p. 4477 - 4480
反应条件
n-butyllithium in diethyl ether
T=-40°C; 0.5 h;
参考文献
Martynov; Sokolov; Aksinenko; Goreva; Epishina; Pushin
Russian Chemical Bulletin, 1998 , vol. 47, # 10 p. 1983 - 1984
反应条件
diethyl sodium phosphite in toluene
T=-8°C;
参考文献
Blackburn, G. Michael; Taylor, Graham E.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 55 - 62
反应条件
1: n-BuLi / tetrahydrofuran / -90 °C
View Scheme
参考文献
Iorga, Bogdan; Eymery, Frederic; Savignac, Philippe
Tetrahedron Letters, 1998 , vol. 39, # 25 p. 4477 - 4480
反应条件
in tetrahydrofuran
Substitution;
参考文献
Zhang, Xin; Weiming, Qiu; Burton, Donald J.
Tetrahedron Letters, 1999 , vol. 40, # 14 p. 2681 - 2684
反应条件
in toluene
T=-35 - 25°C;
参考文献
Blackburn, G. Michael; Taylor, Graham E.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 55 - 62
参考文献
Blackburn, G. Michael; Taylor, Graham E.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 55 - 62
反应条件
perchloryl fluoride; potassium tert-butylate in toluene
0.833333 h; temperature below 22 deg C;
参考文献
McKenna, Charles E.; Shen, Pei-de
Journal of Organic Chemistry, 1981 , vol. 46, # 22 p. 4573 - 4576
