四乙基二氟亚甲基二膦酸酯合成路线 （共 20 条）
反应条件
trimethylsilyl bromide 18 h; Ambient temperature;
参考文献
Hamilton, Chris J.; Roberts, Stanley M.; Shipitsin, Alexander
Chemical Communications, 1998 , # 10 p. 1087 - 1088
反应条件
sodium hydroxide in water
参考文献
Burton, D. J.; Pietrzyk, D. J.; Ishihara, T.; Fonong, T.; Flynn, R. M.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 617 - 626
反应条件
lithium diisopropyl amide in tetrahydrofuran
1.) -70 deg C, 1 h, 2.) -70 deg C, 1 h;
参考文献
Shipitsin, Alexander V.; Victorova, Lyubov S.; Shirokova, Elena A.; Dyatkina, Natalya B.; Goryunova, Lyudmila E.; Beabealashvilli, Robert Sh; Hamilton, Cliris J.; Roberts, Stanley M.; Krayevsky, Alexander
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 8 p. 1039 - 1050
反应条件
1: (EtO)2P(O)CF2Br With tert.-butyl lithium
T=-78°C;
2: 1,2:5,6-di-O-isopropylidene-α-D-ribo-1,5-hexofuranos-3-ulose T=-78 - 0°C;
参考文献
Lopin, Chrystel; Gautier, Arnaud; Gouhier, Geraldine; Piettre, Serge R.
Journal of the American Chemical Society, 2002 , vol. 124, # 49 p. 14668 - 14675
参考文献
Blackburn, G. Michael; Taylor, Graham E.
Journal of Organometallic Chemistry, 1988 , vol. 348, p. 55 - 62
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-70°C; 1 h;
参考文献
Blackburn, G. Michael; Brown, David; Martin, Stephen J.; Parratt, Martin J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 181 - 186
参考文献
Obayashi, Michio; Ito, Eiji; Matsui, Kiyohide; Kondo, Kiyosi
Tetrahedron Letters, 1982 , vol. 23, # 22 p. 2323 - 2326
参考文献
Burton, Donald J.; Flynn, Richard M.
Journal of Fluorine Chemistry, 1980 , vol. 15, p. 263 - 266
反应条件
sodium dibutyl phosphite in hexane
T=-40°C;
参考文献
Blackburn, G. Michael; England, David A.; Kolkmann, Friedrich
Journal of the Chemical Society, Chemical Communications, 1981 , # 17 p. 930 - 932
参考文献
Burton,D.J.; Ishihara,T.
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 121
