in THF-d8 (tetrahydrofuran-d8) THF-d8 is condensed into an NMR tube contg. the alkoxy complex and triphenylsilane (drybox, Ar). The tube is removed from liquid N2, and spectra are taken at different temps. Products are formed after warming to 23°C.; NMR;
参考文献
Rappoli, Brian J.; Janik, Thomas S.; Churchill, Melvyn Rowen; Thompson, Jeffrey S.; Atwood, Jim D.
Organometallics, 1988 , vol. 7, p. 1939 - 1944
