1: 77 percent / NaH / dimethylformamide; various solvent(s) / 24 h / 20 °C
2: 68 percent / PCC; Hyflo Super Cel(R) / CH2Cl2 / 3 h / 20 °C
View Scheme
参考文献
Hornillo-Araujo, Ana R.; Burrell, Adam J.M.; Aiertza, Miren K.; Shibata, Takayuki; Hammond, David M.; Edmont, Dolores; Adams, Harry; Margison, Geoffrey P.; Williams, David M.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 9 p. 1723 - 1729
1: 5-benzyloxy-1-pentanal; diazomethyl-trimethyl-silane With triphenylphosphine; isopropyl alcohol; Wilkinson's catalyst in tetrahydrofuran
T=20°C;
2: pyrocatecholborane in tetrahydrofuran
3: With NaBO3 in 1,4-dioxane; water
T=20°C; 3 h;
参考文献
Lebel, Helene; Ladjel, Chehla
Journal of Organometallic Chemistry, 2005 , vol. 690, # 23 p. 5198 - 5205
