acetyl chloride in benzene soln. placed in a pressure tube fitted with a Teflon stopcock, degassed (vac.), acetyl chloride distilled onto the soln., stirred (1 h); solvent removed by vac. distillation; relation of yield to by-product yield depending on the purity of CH3COCl used and on the care of work up;
参考文献
Bernard, Karen A.; Atwood, Jim D.
Organometallics, 1989 , vol. 8, p. 795 - 800