2,2,4,4-四(三氟甲基)-1,3-二硫杂环丁烷合成路线 （共 43 条）
参考文献
Desjardins,C.D.; Passmore,J.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 3136 - 3146
反应条件
triphenylphosphine in xylene
1 h; Ambient temperature; Product distribution;
参考文献
Elsaesser, Andreas; Sundermeyer, Wolfgang
Chemische Berichte, 1985 , vol. 118, # 11 p. 4553 - 4560
参考文献
E. I. Du Pont de Nemours & Co.
Patent: US3069396 , 1962 ;
C.A., 1963 , vol. 58, p. 10325
反应条件
tri-phenylphosphine sulphide
T=110°C; 12 h; Product distribution;
参考文献
Elsaesser, Andreas; Sundermeyer, Wolfgang
Chemische Berichte, 1985 , vol. 118, # 11 p. 4553 - 4560
反应条件
T=180°C; Product distribution;
参考文献
Elsaesser, Andreas; Sundermeyer, Wolfgang
Chemische Berichte, 1985 , vol. 118, # 11 p. 4553 - 4560
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.1, page 48 - 56
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.1, page 48 - 56
反应条件
bromine; cesium fluoride in N,N-dimethyl-formamide
T=20°C; 15 h; Yield given;
参考文献
Postovoi, S. A.; Vol'pin, I. M.; Delyagina, N. I.; Galakhov, M. V.; Zeifman, Yu. V.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 6.2 p. 1261 - 1264
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 6 p. 1380 - 1383
反应条件
potassium fluoride in N,N-dimethyl-formamide
at 20°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.5.1.1, page 1 - 14
反应条件
acetic anhydride
at 600°C, with acetic anhydride vapor;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.5.1.1, page 1 - 14
