3-(3-甲氧基苯基)-哌啶合成路线 （共 15 条）
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in methanol P=2844.3 Torr; 3 h;
参考文献
Grayson, Neile A.; Bowen, Wayne D.; Rice, Kenner C.
Heterocycles, 1992 , vol. 34, # 12 p. 2281 - 2292
反应条件
hydrogenchloride; sodium hydroxide; PtO2 in methanol
参考文献
US4719219 A1, ;
US 4719219 A
反应条件
1: 76.2 percent / <(C6H5)3P>2NiCl2 2: 90.7 percent / H2, concd. HCl / PtO2 / methanol / 3 h / 2844.3 Torr View Scheme
参考文献
Heterocycles, , vol. 34, # 12 p. 2281 - 2292
反应条件
1: 76.2 percent / <(C6H5)3P>2NiCl2 2: 90.7 percent / H2, concd. HCl / PtO2 / methanol / 3 h / 2844.3 Torr View Scheme
参考文献
Heterocycles, , vol. 34, # 12 p. 2281 - 2292
反应条件
sodium amalgam; sodium salt of phosphorous acid in methanol T=20°C; 2 h;
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
反应条件
sodium amalgam; sodium salt of phosphorous acid in methanol T=20°C; 2 h;
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
反应条件
1: triethylamine / CH2Cl2 2: acetone 3: tetrahydrofuran / 2 h / 20 °C 4: Et3SiH; boron trifluoride etherate / CH2Cl2 / 4 h / 0 °C 5: Na/Hg; sodium phosphate / methanol / 2 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
反应条件
1: acetone 2: tetrahydrofuran / 2 h / 20 °C 3: Et3SiH; boron trifluoride etherate / CH2Cl2 / 4 h / 0 °C 4: Na/Hg; sodium phosphate / methanol / 2 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
反应条件
1: tetrahydrofuran / 2 h / 20 °C 2: Et3SiH; boron trifluoride etherate / CH2Cl2 / 4 h / 0 °C 3: Na/Hg; sodium phosphate / methanol / 2 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
反应条件
1: acetone 2: tetrahydrofuran / 2 h / 20 °C 3: Et3SiH; boron trifluoride etherate / CH2Cl2 / 4 h / 0 °C 4: Na/Hg; sodium phosphate / methanol / 2 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 68, # 6 p. 1173 - 1183
