反应条件
1: With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate in decane; dichloromethane
T=-20°C; 68 h;
2: With sodium hydroxide; sodium chloride
T=20°C; 2 h;
3: With hydrogenchloride in dichloromethane
T=20°C; 2 h;
参考文献
Paju, Anne; Laos, Marit; Jogi, Artur; Paeri, Malle; Jaeaelaid, Raissa; Pehk, Tonis; Kanger, Tonis; Lopp, Margus
Tetrahedron Letters, 2006 , vol. 47, # 26 p. 4491 - 4493