1,3-二甲基-2-咪唑啉酮合成路线 (共 79 条)
反应条件
phosphate buffer pH 7.4 T=37°C; 6.5 h;
参考文献
Saari, Walfred S.; Schwering, John E.; Lyle, Paulette A.; Smith, Steven J.; Engelhardt, Edward L.
Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 97 - 101
反应条件
methanol; nickel T=100°C; P=51485.6 - 102971 Torr; Hydrogenation;
反应条件
in chloroform 0.5 h; Ambient temperature;
参考文献
Rajca, Andrzej; Grobelny, Damian; Witek, Stanislaw; Zbirovsky, Miroslav
Synthesis, 1983 , # 12 p. 1032 - 1033
反应条件
1: 79.6 percent / HCl / ethyl acetate / 3 h / Ambient temperature 2: 14.4 percent / phosphate buffer pH 7.4 / 6.5 h / 37 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 1 p. 97 - 101
反应条件
1: With citric acid in dichloromethane 2: in aq. phosphate buffer; hexadeuterioacetone; water-d2 T=37°C; pH=7.4; Inert atmosphere;
参考文献
Macromolecules, , vol. 46, # 13 p. 5157 - 5166
反应条件
toluene-4-sulfonic acid in toluene 80 h; Heating;
参考文献
Tsuchiya, Yukiko; Kumamoto, Takuya; Ishikawa, Tsutomu
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8504 - 8505
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 317 - 319
反应条件
in chloroform-d1 20 h; Ambient temperature;
参考文献
Corriu, R. J. P.; Lanneau, Gerard F.; Mehta, V. D.
Journal of Organometallic Chemistry, 1991 , vol. 419, # 1 p. 9 - 26
反应条件
potassium carbonate in benzene 1.) ice bath, 2 h; 2.) room temp., overnight;
参考文献
Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, , vol. 39, # 10 p. 929 - 932
反应条件
potassium carbonate in benzene 2 h;
参考文献
Journal of Molecular Structure, , vol. 77, p. 239 - 252