802294-64-0合成路线 （共 916 条）
反应条件
tetrachlorosilane; benzene und Erhitzen des Reaktionsprodukts mit Pyrrol und Natriumacetat auf 180grad;
参考文献
Jur'ew; Eljakow
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 2350,2351;engl.Ausg. S.2627,2628
反应条件
(i) 4-dimethylamino-but-3-yn-2-one, THF, (ii) /BRN= 605259/; Multistep reaction;
参考文献
Neuenschwander,M. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 2428 - 2436
反应条件
1: With (NH4)2S2O8; sulfuric acid; silver nitrate in water T=60 - 70°C; Inert atmosphere; 2: With ammonium hydroxide in water pH=7; Cooling with ice;
参考文献
SANOFI-AVENTIS
Patent: US2011/34452 A1, 2011 ;
Location in patent: Page/Page column 34 ;
反应条件
(NH4)2S2O8; sulfuric acid; silver nitrate in water T=50 - 75°C; 0.833333 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2007/78136 A1, 2007 ;
Location in patent: Page/Page column 70-71 ;
US 20070078136 A1
反应条件
1: With (NH4)2S2O8; sulfuric acid; silver nitrate in water T=60 - 70°C; Inert atmosphere; 2: With ammonium hydroxide in water pH=7; Cooling with ice;
参考文献
SANOFI-AVENTIS
Patent: US2011/34452 A1, 2011 ;
Location in patent: Page/Page column 34 ;
反应条件
methanol; lead (IV)-propionate T=110°C;
参考文献
Reilly Tar and Chem. Corp.
Patent: US2502174 , 1947 ;
参考文献
Goldschmidt; Minsinger
Chemische Berichte, 1954 , vol. 87, p. 956,958, 963
参考文献
Canadian Journal of Chemistry, , vol. 62, # 10 p. 1922 - 1925
反应条件
carbon monoxide; oxygen; trifluoroacetic acid; palladium on activated charcoal; copper dichloride T=75°C; Hydroxylation; P=56887.8 Torr; 18 h;
参考文献
Shen, Chengyu; Garcia-Zayas, Eduardo A.; Sen, Ayusman
Journal of the American Chemical Society, 2000 , vol. 122, # 17 p. 4029 - 4031
反应条件
dihydrogen peroxide in water T=20°C; Irradiation; Further byproducts given;
参考文献
Ogata, Yoshiro; Tomizawa, Kohtaro; Takagi, Kaoru
Canadian Journal of Chemistry, 1981 , vol. 59, p. 14 - 18
