802294-64-0合成路线 （共 916 条）
反应条件
N-bromosuccinmide; sulfuric acid in trifluoroacetic acid T=85°C; 16 h;
参考文献
Zhang, Lian Hao; Duan, Jianxin; Xu, Yuelian; Dolbier Jr., William R.
Tetrahedron Letters, 1998 , vol. 39, # 52 p. 9621 - 9622
参考文献
Hunter; Edgar
Journal of the American Chemical Society, 1932 , vol. 54, p. 2025,2026
参考文献
Varma; Menon
Journal of the Indian Chemical Society, 1933 , vol. 10, p. 592
Chem. Zentralbl., 1934 , vol. 105, # I p. 2105
反应条件
water; 1,2,3-benzenetriol T=200°C;
参考文献
BASF
Patent: DE962428 , 1954 ;
反应条件
1,2,3-benzenetriol T=320°C; und Erwaermen des Reaktionsprodukts mit wss. Natronlauge;
参考文献
BASF
Patent: DE962429 , 1955 ;
反应条件
1,2,3-benzenetriol T=320°C;
参考文献
BASF
Patent: DE962429 , 1955 ;
反应条件
in not given prepn. from ZnCO3 and carboxylic acid in molar ratio 1:2;
参考文献
Czakis-Sulikowska; Radwannska-Doczekalska; Markiewicz; Pietrzak
Journal of Thermal Analysis and Calorimetry, 2008 , vol. 93, # 3 p. 789 - 794
反应条件
in water Zn(OH)2 dissolved in stoich. amt. of carboxylic acid; evapd. up to crystn. on water bath and then at room temp.; dried over silica gel;
参考文献
Vlase; Chiriac; Doca
Journal of Thermal Analysis and Calorimetry, 2003 , vol. 72, # 3 p. 839 - 845
反应条件
in neat (no solvent) excess carboxylic acid, repeated vibration milling; not isolated, detd. by IR spectroscopy;
参考文献
Dreveni; Berkesi; Andor; Mink
Inorganica Chimica Acta, 1996 , vol. 249, # 1 p. 17 - 23
反应条件
in propionic acid heating soln. of zinc compd. in propionic acid at 120°C for 2 h in N2 flow; concg. in vac., drying at 70°C in vac.;
参考文献
Kim, Min; Lai, Samson; Laine, Richard M.
Journal of the American Ceramic Society, 2011 , vol. 94, # 10 p. 3308 - 3318
