1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in water T=90 - 100°C; Isomerization; 2.5 h;
参考文献
Wang, Dong; Chen, Dongli; Haberman, John X.; Li, Chao-Jun
Tetrahedron, 1998 , vol. 54, # 20 p. 5129 - 5142
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in water T=100°C; 8 h;
参考文献
Zhang, Fang; Kang, Chunmei; Wei, Yongyi; Li, Hexing
Advanced Functional Materials, 2011 , vol. 21, # 16 p. 3189 - 3197
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
参考文献
Meyer, Christophe; Cossy, Janine
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7861 - 7864
参考文献
Meyer, Christophe; Cossy, Janine
Tetrahedron Letters, 1997 , vol. 38, # 45 p. 7861 - 7864
反应条件
1: 67 percent / Et3N / diethyl ether / 15 h / Ambient temperature 2: 1) (COCl)2, DMSO, 3) Et3N 3: 82 percent / H2, 42percent aq. HBF3 / Raney Ni / ethanol / 16 h / 760 Torr / Ambient temperature View Scheme
参考文献
Kanemasa Asai; Tanaka
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 2 p. 375 - 380
反应条件
1: 39 percent / 1 h / 400 °C / thermolysis study, other conditions, other derivatives 2: 60 percent / diethyl ether / 2 h / 25 °C 3: 85.6 percent / PCC / CH2Cl2 / 2 h / Ambient temperature 4: 93 percent / NaBD4 / tetrahydrofuran / 1 h / Heating 5: 93.4 percent / 1 h / 400 °C View Scheme
参考文献
Ranganathan, S.; Kumar, Raaj; Maniktala, V.
Tetrahedron, 1984 , vol. 40, # 7 p. 1167 - 1178
反应条件
1: KHSO4 2: 1) O2, 2) H2 / 2) Raney-Ni / 1) 50 deg C, toluene, 2) 100 deg C, 16 MPa View Scheme
参考文献
Blau, K.; Voerkel,V.; Willecke, L.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 1 p. 29 - 34
反应条件
cobalt(II) chloride in acetonitrile T=80°C; 3 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
lithium aluminium tetrahydride; bis(cyclopentadienyl)titanium dichloride 1.) THF, 6 h, reflux; 2.) hydrolysis; Yield given. Multistep reaction;
参考文献
Sato, Fumie; Tomuro, Yasuji; Ishikawa, Hiroaki; Oikawa, Takeshi
Chemistry Letters, 1980 , p. 103 - 106
反应条件
1.1: amino lipase PS / 70 h / 20 °C / Enzymatic reaction 2.1: sodium hydride / tetrahydrofuran; mineral oil / 1.25 h / 20 °C / Inert atmosphere 2.2: 24 h / Inert atmosphere; Reflux 3.1: sec.-butyllithium / diethyl ether; hexane; cyclohexane / 1 h / -78 °C / Inert atmosphere 3.2: 2 h / -78 °C / Inert atmosphere 4.1: cesium fluoride / dichloromethane; water / 16 h / 20 °C 5.1: tetrahydrofuran / 2 h / 20 °C 6.1: dihydrogen peroxide; sodium hydroxide / water / 0 - 20 °C 7.1: Jone's reagent / acetone / 0 - 20 °C 8.1: chlorosulfonic acid / dichloromethane / 0.75 h / 20 °C 9.1: sodium acetate / ethanol / 15 h / Reflux 9.2: 20 h / 20 °C / 760.05 Torr View Scheme
参考文献
Roesner, Stefan; Casatejada, Javier Mansilla; Elford, Tim G.; Sonawane, Ravindra P.; Aggarwal, Varinder K.
Organic Letters, 2011 , vol. 13, # 21 p. 5740 - 5743
