1-苯基-3-丁烯-1-醇合成路线 （共 285 条）
反应条件
1: anhydrous iron chloride; chloramine-T / dichloromethane / 20 °C / Inert atmosphere
2: indium / dichloromethane / 20 °C / Inert atmosphere
View Scheme
参考文献
Srivastava, Vishnu P.; Patel, Rajesh; Yadav, Lal Dhar S.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 5 p. 695 - 700
反应条件
bis(benzonitrile)palladium(II) dichloride; tin(ll) chloride in water
48 h; Ambient temperature; Yield given;
参考文献
Masuyama, Yoshiro; Nimura, Yumiko; Kurusu, Yasuhiko
Tetrahedron Letters, 1992 , vol. 33, # 43 p. 6477 - 6478
反应条件
in dichloromethane
Heatingvariation of aldehydes, variation of siliconates;
参考文献
Hosomi, Akira; Kohra, Shinya; Ogata, Koichiro; Yanagi, Toshiharu; Tominaga, Yoshinori
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2415 - 2420
反应条件
n-butyllithium; zinc dibromide
multistep reaction: 1.) THF, pentane, 0 deg C, 15 min, 2.) THF, room temperature, 1 h; formation of allylzinc reagent, its reaction with carbonyl compounds; reaction of various substituted allylzinc reagents with electrophiles; Product distribution;
参考文献
Jones, Philip; Knochel, Paul
Journal of Organic Chemistry, 1999 , vol. 64, # 1 p. 186 - 195
反应条件
catalyst: Pd(OAc)2-triphenylphosphine in dimethyl sulfoxide
under Ar; DMSO, CH2CHCH2Cl, allylstannane, PhCHO added to mixt. of Pd(OAc)2 and PPh3 (molar ratio 11:10:5:1:2); heated at 100°C for 20 h; treated with water; extd. with ether; distd. under reduced pressure; detd. by GC;
参考文献
Kiji, Jitsuo; Okano, Tamon; Nomura, Takaaki; Saiki, Kayoko; Sai, Torei; Tsuji, Jiro
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 10 p. 1939 - 1945
反应条件
tin; benzaldehyde in tetrahydrofuran; water
0.5 h; Ambient temperaturesonication;
参考文献
Petrier, C.; Einhorn, J.; Luche, J. L.
Tetrahedron Letters, 1985 , vol. 26, # 11 p. 1449 - 1452
参考文献
Barluenga, Jose; Fananas, Francisco J.; Villamana, Jorge; Yus, Miguel
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2685 - 2692
反应条件
hydrogenchloride
T=25°C; other aldehydes and ketones, other alkylvinyltin halides;
参考文献
Gambaro, Alessandro; Peruzzo, Valerio; Plazzogna, Gualtiero; Tagliavini, Guiseppe
Journal of Organometallic Chemistry, 1980 , vol. 197, # 1 p. 45 - 50
反应条件
pentacarbonyliron(0) in benzene
Barbier-type reaction; 2 h; Heating;
参考文献
Vasil'Eva; Mysova; Chakhovskaya; Terent'Ev
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 7 p. 1014 - 1017
反应条件
1: 65 percent / O3; O2 / hexane; CH2Cl2 / -78 °C
2: 13 percent / SnCl4 / CH2Cl2 / -78 °C
View Scheme
参考文献
Dussault, Patrick H.; Lee, Hyung-Jae; Liu, Xuejun
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 17 p. 3006 - 3013
