1,2,3,4-四氢-6-羟基-1-萘羧酸合成路线 （共 32 条）
反应条件
nickel; sodium carbonate
T=75°C; P=128714 Torr; Hydrogenation;
参考文献
Dauben et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1393,1397
反应条件
1: aluminium chloride
2: aqueous hydrobromic acid; acetic acid
3: sodium
View Scheme
参考文献
Price; Enos; Kaplan
Journal of the American Chemical Society, 1947 , vol. 69, p. 2261,2263
反应条件
1: aqueous hydrobromic acid; acetic acid
2: sodium
View Scheme
参考文献
Price; Enos; Kaplan
Journal of the American Chemical Society, 1947 , vol. 69, p. 2261,2263
反应条件
1: aluminium chloride
2: aqueous hydrobromic acid; acetic acid
3: sodium
View Scheme
参考文献
Price; Enos; Kaplan
Journal of the American Chemical Society, 1947 , vol. 69, p. 2261,2263
参考文献
Price; Enos; Kaplan
Journal of the American Chemical Society, 1947 , vol. 69, p. 2261,2263
反应条件
1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
2: acetonitrile-D3; water-d2 / |Photolysis
3: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
4: silver(l) oxide / acetonitrile / 60 °C
5: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: water / acetonitrile-D3 / |Photolysis
2: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
3: silver(l) oxide / acetonitrile / 60 °C
4: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: potassium permanganate / benzene / |Reflux; |Dean-Stark
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
3: acetonitrile-D3; water-d2 / |Photolysis
4: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
5: silver(l) oxide / acetonitrile / 60 °C
6: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
2: silver(l) oxide / acetonitrile / 60 °C
3: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: acetonitrile / |Reflux
2: lithium hexamethyldisilazane
3: hydrogen; platinum on activated charcoal / methanol
4: methanesulfonic acid; phosphorous pentoxide
5: AlCl3, aluminium chloride / benzene / |Reflux
6: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
7: silver(l) oxide / acetonitrile / 60 °C
8: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
