3,3,5,5-四-叔-丁基-4,4-芪醌合成路线 (共 30 条)
反应条件
in diethyl ether
0.666667 h;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1984 , vol. 49, # 17 p. 3046 - 3050
反应条件
1: 70 percent / Cu(II)Cl2 / acetonitrile / 1 h / 20 °C / decomposition in presence of Cu(I)Cl is also investigated
2: air
View Scheme
参考文献
Maumy, Michel; Capdevielle, Patrice
Tetrahedron, 1993 , vol. 49, # 34 p. 7455 - 7462
反应条件
potassium acetate in water
T=100°C; 0.5 h;
参考文献
Barton, Benita; Logie, Catherine G.; Schoonees, Barbara M.; Zeelie, Bernard
Organic Process Research and Development, 2005 , vol. 9, # 1 p. 62 - 69
反应条件
1: 98 percent / acetone / 0.5 h / 20 °C
2: N-acetylthiourea / acetone / 20 °C
View Scheme
参考文献
Gorbunov, D. B.; Voznesenskii, V. N.; Ershov, V. V.; Nikiforov, G. A.
Russian Chemical Bulletin, 1994 , vol. 43, # 1 p. 93 - 97
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 1 p. 98 - 102
反应条件
methyllithium; silver perchlorate in tetrahydrofuran
T=25°C;
参考文献
Macomber, Roger S.
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2481 - 2483
反应条件
lead dioxide in benzene
72 h; Heating;
参考文献
Colegate, Steven M.; Hewgill, F. Richmond
Australian Journal of Chemistry, 1980 , vol. 33, # 2 p. 351 - 369
参考文献
Gazizov; Ismagilov; Shamsutdinova; Karimova; Sinyashin
Russian Journal of General Chemistry, 2012 , vol. 82, # 2 p. 212 - 216
反应条件
copper(I) oxide; 1-bromonitrobenzene in various solvent(s)
2 h; Heating;
参考文献
Bacon,R.G.R.; Stewart,O.J.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 301 - 308
反应条件
in acetic acid
T=50°C; 15 h;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
反应条件
3,3',5,5'-tetra-tert-butyl-4,4'-diphenoquinone in isopropyl alcohol
T=195°C; 6 h; Product distribution;
参考文献
Mukmeneva; Bukharov; Kadyrova; Zharkova; Gorshunova; Fazlieva
Russian Journal of General Chemistry, 1996 , vol. 66, # 9 p. 1486 - 1489