80937-33-3合成路线 （共 1249 条）
反应条件
in neat (no solvent)
thermal treatment of RbTeF5 in air, 450°C, 3h;
参考文献
Germain, Patrick; Claudy, Pierre; Letoffe, Jean-Marie; Bastide, Jean-Pierre
Materials Research Bulletin, 1988 , vol. 23, p. 1731 - 1738
反应条件
in neat (no solvent)
heating in dry oxygen to 300°C;
参考文献
Ippolitov, E. G.; Tripol'skaya, T. A.; Zhigarnovskii, B. M.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1979 , vol. 24, p. 299 - 301
Zhurnal Neorganicheskoi Khimii, 1979 , vol. 24, p. 539 - 541
反应条件
in neat (no solvent)
silent discharge;;
参考文献
Gmelin Handbook: Cl: MVol., 20, page 68 - 71
反应条件
in neat (no solvent)
Irradiation (UV/VIS); not isolated;;
参考文献
Gmelin Handbook: Cl: SVol.B2, 1, page 315 - 317
反应条件
in neat (no solvent)
glow discharge at temp. of liquid oxygene;;
参考文献
Gmelin Handbook: Cl: SVol.B2, 17, page 349 - 351
反应条件
in solid
Kinetics; O2 activated in a glow discharge; not isolated detected by IR;
参考文献
Morozova, N. P.; Dadashova, E. A.; Yagodovskaya, T. V.; Nekrasov, L. I.
Russian Journal of Physical Chemistry, 1989 , vol. 63, # 7 p. 1095 - 1096
Zhurnal Fizicheskoi Khimii, 1989 , vol. 63, p. 1983 - 1985
反应条件
in neat (no solvent)
Irradiation (UV/VIS); mixt. of Cl2, SO2 and O2 irradiated (>320 nm) at -78°C; distd. into traps (-90, -120, -196°C); O2 pumped off; distd. intotraps (-70, -110, -196°C) by slow warming to room temp.; peroxid e from -70°C trap purified by trap-to-trap distns.; collected in -50°C trap; detd. by IR, Raman;
参考文献
Romano, Rosana M.; Vedova, Carlos O.Della; Beckers, Helmut; Willner, Helge
Inorganic Chemistry, 2009 , vol. 48, # 5 p. 1906 - 1910
反应条件
in neat (no solvent)
Kinetics; byproducts: CH3OH, CH3OD, CO; heated (heating tape) in a Pyrex cell, backing pressure of <1E-5 mbar, 583 K, excess of oxygen; methanol and formaldehyde detected as transient species; not isolated; IR;
参考文献
Harrison, Philip G.; Ashworth, Andrew; Clark, Edward N.; McManus, James
Journal of the Chemical Society, Faraday Transactions, 1990 , vol. 86, # 24 p. 4059 - 4063
反应条件
in neat (no solvent)
reaction of a mixture of Cl2 and O2 (2:1) with Si in a glass tube at red heat; further products;; condensation and fractionation;;
参考文献
Gmelin Handbook: Si: MVol.B, 260, page 704 - 707
反应条件
in neat (no solvent)
reaction of a mixture of Cl2 and O2 (2:1) with Si in a glass tube at red heat; further products;; condensation and fractionation;;
参考文献
Gmelin Handbook: Si: MVol.B, 260, page 704 - 707
