80937-33-3合成路线 （共 1249 条）
反应条件
Kinetics; byproducts: monochlorocyclopentadiene polymer, HCl, Cl2; solvent: THF or toluene; closed ampules (106.6 kPa of O2), shaking (3 h,room temperature); ampules centrifugation, supernatant from THF-pentane crystn. at low temperature; elem. anal.;
参考文献
Russian Journal of General Chemistry, , vol. 66, # 5 p. 701 - 704
反应条件
heating to 300 - 400 °C;; OsO4 is condensed on dry ice/alcohol trap;;
参考文献
Gmelin Handbook: Os: MVol., 31, page 58 - 60
反应条件
in neat (no solvent) O2 passed through Os powder contained in an alumina cell equipped with a gas inlet tube; not isolated, detected by mass spectrometry;
参考文献
Aoyama, S.; Watanabe, K.
Nippon Kagaku Zasshi, 1955 , vol. 76, p. 594 - 596
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Gmelin Handbook: Os: SVol.1, 3.2.1.2.1, page 75 - 76
反应条件
in neat (no solvent) Kinetics; isothermal conditions: MgO preheated under N2 up to 850-1025°C, Cl2-O2 mixt. (Cl2:O2=4) introduced; non-isothermal conditions: MgO in Cl2-O2 (Cl2:O2=4) atmosphere heated to 850-1025°C; monitored by thermogravimetric analysis;
参考文献
Kanari; Gaballah; Allain
Thermochimica Acta, 2000 , vol. 351, # 1-2 p. 131 - 137
反应条件
SO2 in neat (no solvent) very slow absorption of SO2 by MgO up to 230°C, mechanism discussed;; quant. react. to sulfate;;
参考文献
Birnbaum, K.; Wittich, C.
Ber., 1880 , vol. 13, p. 651 - 653
Full Text Show Details
Gmelin Handbook: S: MVol.B1, 132, page 288 - 290
反应条件
in solid heating at 600-900 °C; X-ray diffraction;
参考文献
Crnkovic; Milioli; Pagliuso
Thermochimica Acta, 2006 , vol. 447, # 2 p. 161 - 166
反应条件
in solid Kinetics; byproducts: CO2, H2O; reaction during thermal decomposition of mixture from 25-1000°C, heating rate of 10 deg/min; mixt. of MgCO3; MgSO4; and Fe(OH)2 formed in temp. range 70-200; further decompn. from 200-520 with formn. of Fe2O3; MgO formn. from 520-560 °C; detd. by XRD;
参考文献
Prasad, T. P.
Journal of Thermal Analysis, 1987 , vol. 32, p. 1505 - 1510
反应条件
in neat (no solvent) Au-assisted growth of ZnO by plasma-enhanced MOCVD, O2 and H2 used as carrier gas for Et2Zn, react. time 3 h; vertically aligned nanowires obtained on Si substrate, characterized by SEM, PL spectra and TEM;
参考文献
Zhang, Guoqiang; Nakamura, Atsushi; Aoki, Toru; Temmyo, Jiro; Matsui, Yoshio
Applied Physics Letters, 2006 , vol. 89, # 11 art. no. 113112
反应条件
in hydrogenchloride byproducts: H2O; Bi is dissloved in aq. HCl only in presence of air;;
参考文献
Gmelin Handbook: Bi: MVol., 51, page 138 - 140
反应条件
triethanolamine in benzonitrile Kinetics; Irradiation (UV/VIS); methyl viologen aerated soln. added to the photo-irradiated fullerene soln. containing triethanolamine as electron donor; steady-state UV-vis/NIR monitoring;
参考文献
Konishi, Toshifumi; Fujitsuka, Mamoru; Ito, Osamu
Chemistry Letters, 2000 , # 3 p. 202 - 203
