80937-33-3合成路线 (共 1249 条)
反应条件
in neat (no solvent) Irradiation (UV/VIS); mixt. of Cl2, SO2 and O2 irradiated (>320 nm) at -78°C; distd. into traps (-90, -120, -196°C); O2 pumped off; distd. intotraps (-70, -110, -196°C) by slow warming to room temp.; peroxid e from -70°C trap purified by trap-to-trap distns.; collected in -50°C trap; detd. by IR, Raman;
参考文献
Romano, Rosana M.; Vedova, Carlos O.Della; Beckers, Helmut; Willner, Helge
Inorganic Chemistry, 2009 , vol. 48, # 5 p. 1906 - 1910
反应条件
in neat (no solvent) byproducts: CO2, CO; oxidn. of CS2 with oxygen, mechanism discussed;;
参考文献
Bawn, C. E. H.
Journal of the Chemical Society, 1933 , p. 145 - 151
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Gmelin Handbook: S: MVol.B1, 89, page 197 - 198
反应条件
in solid matrix Irradiation (UV/VIS); 0.5 h white light photolysis at λ >= 220 nm at 12 K, warmed up to 32 K; IR;
参考文献
Green, Martina; Lee, Edward K. C.
Journal of Physical Chemistry, 1986 , vol. 90, # 24 p. 6470 - 6475
反应条件
in neat (no solvent) combustion of S in a calorimetric bomb with O2-pressures of 2.5 to 45 atm;; H2S2O7 and NOHSO4 remaines as residue in bomb, but formation because of content of N2, H2 and H2O of used O2;;
参考文献
Giran, H.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 140, p. 1704 - 1707
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Gmelin Handbook: S: MVol.B1, 74, page 164 - 166
反应条件
in neat (no solvent) byproducts: H2O; explosion of H2S-O2-mixture, mechanism discussed;; product mixture and unburned H2S and O2 obtained;;
参考文献
Taylor, H. A.; Livingston, E. M.
Journal of Physical Chemistry, 1931 , vol. 35, p. 2676 - 2683
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Gmelin Handbook: S: MVol.B1, 22, page 47 - 49
反应条件
in gaseous matrix Kinetics; oxidn. of H2 in presence of SO2 (up to 20percent) at 773 K, 400 Torr, N2 carrier gas, semi-state method (monitoring of react. by pressure change);
参考文献
Chamboux, J.; Viossat, V.; Jorand, F.; Sahetchian, K.
Journal de Chimie Physique et de Physico-Chimie Biologique, 1985 , vol. 82, # 5 p. 499 - 504
参考文献
Schoenherr, S.; Schrader, R.; Mahlitz, P.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1969 , vol. 365, p. 262 - 268
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Gmelin Handbook: S: SVol.3, 3.1.1.5, page 257 - 257
参考文献
Dudley, B.
Chem. Metall. Eng., 1915 , vol. 13, p. 221 - 226
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Dudley, B.
Chem. Metall. Eng., 1915 , vol. 13, p. 303 - 308
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Gmelin Handbook: Ni: MVol.AI, 3.2.1, page 451 - 456
反应条件
Kinetics; iron oxide formed acts as catalyst for SO3 formation;
参考文献
Gmelin Handbook: S: MVol.A2, 2.3.1, page 286 - 300
参考文献
Gmelin Handbook: S: MVol.A2, 2.3.1, page 286 - 300