1: 98 percent / NaBH4 / methanol / 24 h / Heating
2: 58 percent / CHCl3 / 22 h / Heating
3: H2 / tris(triphenylphosphine)rhodium chloride / benzene / 14 h / 20 °C
4: 96 percent / sodium acetate / 0.5 h / 100 °C
5: 97 percent / H2 / tris(triphenylphosphine)rhodium chloride / benzene / 40 h / 20 °C
6: chromic anhydride / acetic acid; H2O / 24 h / 70 °C
7: 98 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 0.75 h / Heating
8: 78 percent / silver acetate / 0.25 h / Heating
9: aq. NH4OH / acetone / 24 h / 20 °C
View Scheme
参考文献
Gupta, Dharmendra N.; Hodge, Philip; Khan, Naeem
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 689 - 696
1: 86 percent / triethylamine / dimethylsulfoxide / 4 h / Ambient temperature
2: 76 percent / 10percent aq. NaOH / dioxane / 2 h / 80 °C
3: 86 percent / quinoline / 120 °C
View Scheme
参考文献
Bingham, Steve J.; Tyman, John H. P.; Malik, K. M. A.; Hibbs, David E.; Hursthouse, Michael B.
Journal of Chemical Research, Miniprint, 1998 , # 9 p. 2465 - 2496
