in diethyl ether byproducts: MePhEtSiH; EtLi in ether was added to an equimolar amt. of silane, room temp., N2 atm.; hydrolysis, extn. (ether), evapn., not sep., detected with NMR spectra and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50
in diethyl ether byproducts: (+)-MePhEtSiOMe; EtLi and EtBr in ether were added to an equimolar amt. of silane, room temp., 12 h, N2 atm.; not sep., detected with NMR spectra and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50
in diethyl ether byproducts: MePhEtSiOMe; EtLi in ether was added to an equimolar amt. of silane, room temp., 3 h, N2 atm.; not sep., detected with NMR spectra and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50
in diethyl ether byproducts: (+)-MePhEtSiH; EtLi and EtBr in ether were added dropwise to an equimolar amt. of silane, room temp., 12 h, N2 atm.; filtration, evapn., not sep., detected with NMR spectra and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50
in diethyl ether EtLi and EtBr in ether were added dropwise to an equimolar amt. of silane, room temp., 24 h, N2 atm.; filtration, evapn., not sep. detected with NMR specra and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50
