1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.166667 h; Inert atmosphere;
2: diethyl chlorophosphate in tetrahydrofuran; hexane
1 h;
参考文献
Ha, Young-Geun; Emery, Jonathan D.; Bedzyk, Michael J.; Usta, Hakan; Facchetti, Antonio; Marks, Tobin J.
Journal of the American Chemical Society, 2011 , vol. 133, # 26 p. 10239 - 10250
1: o-bromodiphenylphosphine With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; Metallation;
2: diethyl chlorophosphate T=20°C; Substitution; 4 h; Further stages.;
参考文献
Ellis, Dianne D.; Harrison, Gayle; Guy Orpen; Phctmung, Hirihattaya; Pringle, Paul G.; Dcvries, Johannes G.; Oevering, Henk
Journal of the Chemical Society, Dalton Transactions, 2000 , # 5 p. 671 - 675