反应条件
1: methyl vinyl ketone With 2,2,6,6-tetramethyl-piperidine; n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.333333 h; Inert atmosphere;
2: diethyl chlorophosphate in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Banuelos, Patrcia; Garcia, Jesus M.; Gomez-Bengpa, Enrique; Herrero, Ada; Odriozola, Jose M.; Oiarbide, Mikel; Palomo, Claudio; Razkin, Jesus
Journal of Organic Chemistry, 2010 , vol. 75, # 5 p. 1458 - 1473