2-甲基-1-丁烯-3-酮合成路线 （共 116 条）
参考文献
Ogloblin
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 2157
Chem.Abstr., 1949 , p. 3777
反应条件
ethanol; magnesium oxide; zinc oxide
T=400°C;
参考文献
Hart; Levitt
Journal of Organic Chemistry, 1959 , vol. 24, p. 1261,1266
反应条件
ozone in chloroform-d1
T=-50°C; Title compound not separated from byproducts;
参考文献
Griesbaum, Karl; Greunig, Hans-Joachim; Volpp, Willi; Jung, In-Chan
Chemische Berichte, 1991 , vol. 124, # 4 p. 947 - 956
反应条件
ethanol; iron(III) chloride; zinc(II) chloride
参考文献
Bahner et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 682
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Tamura; Yamasaki
Yakugaku Zasshi, 1956 , vol. 76, p. 915
Chem.Abstr., 1957 , p. 2782
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol
T=80°C;
参考文献
Neely, Jamie M.; Rovis, Tomislav
Journal of the American Chemical Society, 2014 , vol. 136, # 7 p. 2735 - 2738
反应条件
methanol; potassium hydroxide
参考文献
Chapurlat,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2446 - 2450
反应条件
1: NaOMe / 174 - 206 °C
2: NaOEt / ethanol
View Scheme
参考文献
Lacey,R.N.
Journal of the Chemical Society, 1960 , p. 1625 - 1633
反应条件
1: chloroform; triethylamine; hydrogen sulfide / -15 °C
2: aqueous NaOH-solution
View Scheme
参考文献
Thiel et al.
Justus Liebigs Annalen der Chemie, 1958 , vol. 619, p. 137,143
反应条件
1: 1.) BuLi, LDA / 1.) hexane, diethylether, -60 deg C, 15 min, 2.) 5 min
2: 1.)acetic acid, TsNHNH2, 2.) NaBH3CN / 1.) RT, 1 h, 2a.) RT, 1 h, 2b.) 70 deg C, 2 h
View Scheme
参考文献
Baeckstroem, Peter; Li, Lanna
Synthetic Communications, 1990 , vol. 20, # 10 p. 1481 - 1485
反应条件
hydroquinone
T=120°C;
参考文献
Westfahl; Gresham
Journal of the American Chemical Society, 1955 , vol. 77, p. 936,938
