1,1,2,2-四甲基乙硅烷合成路线 (共 19 条)
参考文献
Journal of the Chemical Society, Faraday Transactions, , vol. 89, # 3 p. 411 - 418
反应条件
Ambient temperatureIrradiationvarious reaction times, effects of radical scavengers; Product distributionQuantum yield;
参考文献
Journal of the Chemical Society - Faraday Transactions, , vol. 93, # 6 p. 1071 - 1078
反应条件
in cyclohexane byproducts: H2, CO; N2-atmosphere; 2 equiv. of disilane, stirring (20 h); filtration, pumping off of volatiles (1 Torr, room temp.), dissoln. in toluene, crystn. on cooling (-80°C), decantation, drying (vac.);
参考文献
Kerber; Pakkanen
Inorganica Chimica Acta, 1979 , vol. 37, p. 61
反应条件
Pd0(tris(tert-butyl)phosphine)2; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 96 h; Inert atmosphere;
参考文献
Lesbani, Aldes; Kondo, Hitoshi; Sato, Jun-Ichi; Yamanoi, Yoshinori; Nishihara, Hiroshi
Chemical Communications, 2010 , vol. 46, # 41 p. 7784 - 7786
反应条件
in toluene
Ar-atmosphere; stirring at 25°C for 5 d;
参考文献
Karch, Ralf; Schubert, Ulrich
Inorganica Chimica Acta, 1997 , vol. 259, # 1-2 p. 151 - 160
反应条件
Ni(PEt3)2Cl2 in toluene
Heating;
参考文献
Sanji, Takanobu; Ishiwata, Hiroyuki; Kaizuka, Tomoyoshi; Tanaka, Masato; Sakurai, Hideki; Nagahata, Ritsuko; Takeuchi, Kazuhiko
Chemistry Letters, 2005 , vol. 34, # 8 p. 1130 - 1131
反应条件
aluminium trichloride
T=20°C; 14 h;
参考文献
Razuvaev, G. A.; Brevnova, T. N.; Semenov, V. V.; Sevast'yanova, E. I.; Khorshev, S. Ya.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 10 p. 2267 - 2747,1835 - 1840
反应条件
iodine in dichloromethane
参考文献
Triplett,K.; Curtis,M.D.
Journal of Organometallic Chemistry, 1976 , vol. 107, p. 23 - 32
参考文献
Okinoshima,H. et al.
Journal of Organometallic Chemistry, 1975 , vol. 86, p. C27 - C30