2,2,4,4-四甲基-3-戊酮合成路线 (共 175 条)
参考文献
Midland,M.M.
Journal of Organic Chemistry, 1975 , vol. 40, # 15 p. 2250 - 2252
反应条件
diethyl ether; copper(l) chloride
参考文献
Petrow et al.
Doklady Akademii Nauk SSSR, 1953 , vol. 91, p. 857,859
Chem.Abstr., 1954 , p. 10575
反应条件
1: Li, liq. NH3 / diethyl ether 2: HCl, AcOH / dioxane 3: Zn / acetonitrile / Heating View Scheme
参考文献
Hartzler,H.D.
Journal of the American Chemical Society, 1971 , vol. 93, p. 4527 - 4531
反应条件
in N-dodecane T=30°C; 0.5 h; Irradiationalso in other solvents (solvent viscosity dependence); Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 104, # 1 p. 225 - 229
反应条件
sodium tetrahydroborate; Amberlyst-15(H+) in tetrahydrofuran 0.116667 h; Ambient temperature;
参考文献
Caycho, Juana Robles; Tellado, Fernando Garcia; De Armas, Pedro; Tellado, Jose Juan Marrero
Tetrahedron Letters, 1997 , vol. 38, # 2 p. 277 - 280
反应条件
titanium tetrachloride; lithium in THF-d8 (tetrahydrofuran-d8) T=20°C; McMurry reaction; 24 h; Further byproducts.;
参考文献
Villiers, Claude; Ephritikhine, Michel
Chemistry - A European Journal, 2001 , vol. 7, # 14 p. 3043 - 3051
反应条件
titanium tetrachloride; lithium in THF-d8 (tetrahydrofuran-d8) T=20°C; McMurry reaction; 24 h; Further byproducts.;
参考文献
Villiers, Claude; Ephritikhine, Michel
Chemistry - A European Journal, 2001 , vol. 7, # 14 p. 3043 - 3051
反应条件
in benzene T=24.75°C;
参考文献
Maclin, Keith M.; Richey Jr., Herman G.
Journal of Organic Chemistry, 2002 , vol. 67, # 13 p. 4602 - 4604
反应条件
titanium tetrachloride; lithium in tetrahydrofuran T=20°C; McMurry reaction; 24 h; Product distribution; Further Variations:Solvents;
参考文献
Villiers, Claude; Ephritikhine, Michel
Chemistry - A European Journal, 2001 , vol. 7, # 14 p. 3043 - 3051
参考文献
Helaja, T. Tuulamari; Loefgren, Barbro; Hase, Tapio
Acta Chemica Scandinavica, 1999 , vol. 53, # 5 p. 352 - 355