2,2,4,4-四甲基-3-戊酮合成路线 (共 175 条)
反应条件
diethyl ether T=-35°C;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 2806,2811
反应条件
in tetrahydrofuran T=0°C; 0.5 h;
参考文献
De Las Heras, Maria A.; Vaquero, Juan J.; Garcia Navio, Jose L.; Alvarez-Builla, Julio
Tetrahedron, 1996 , vol. 52, # 45 p. 14297 - 14310
反应条件
diethyl ether; 1,1-dimethylethylmagnesium chloride; copper(l) chloride 3-taegiges Behandeln des Reaktionsprodukts mit Wasser-Dampf;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 57, p. 566
Journal of the American Chemical Society, , vol. 60, p. 2028
Journal of the American Chemical Society, , vol. 71, p. 4142
反应条件
1,2-dibromo-1,1,2,2-tetrachloroethane; potassium carbonate; di-p-methoxyphenyl telluride in chloroform 15 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 21, p. 1785 - 1788
反应条件
1: 4-tert-butyl-4-hydroxy-2,2,5,5-tetramethylhexan-3-one With methyllithium in tetrahydrofuran; diethyl ether T=-40°C; 0.166667 h; Inert atmosphere; 2: dicyclopropyl-methanone in tetrahydrofuran; diethyl ether T=-40 - 20°C; Inert atmosphere;
参考文献
Knorr; Boehrer; Schubert
Chemistry - A European Journal, 2012 , vol. 18, # 24 p. 7506 - 7515
反应条件
reusable unsupported rhenium nanocrystalline particle in neat (no solvent) T=180°C; 10 h; Green chemistry;
参考文献
Yi, Jing; Miller, Jeffrey T.; Zemlyanov, Dmitry Y.; Zhang, Ruihong; Dietrich, Paul J.; Ribeiro, Fabio H.; Suslov, Sergey; Abu-Omar, Mahdi M.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 3 p. 833 - 836
Angew. Chem., 2013 , vol. 126, # 03 p. 852 - 855,4
反应条件
oxygen; methylene blue in chloroform Irradiationother solvents, thioketone concentrations, and sources of singlet oxygen; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 47, # 1 p. 127 - 131
参考文献
Journal of the American Chemical Society, , vol. 55, p. 4156
Journal of the American Chemical Society, , vol. 55, p. 3736
反应条件
sodium; pentane und Oxidieren der bei 150-165grad siedenden Fraktion mit HNO3;
参考文献
Journal of the American Chemical Society, , vol. 67, p. 143
Journal of Research of the National Bureau of Standards (United States), , vol. 38, p. 391
Chem. Zentralbl., , vol. 118, p. 5291
参考文献
Dubois, Jacques-Emile; Zhang, Ben Li; Lion, Claude
Tetrahedron, 1981 , vol. 37, # 24 p. 4189 - 4194